By Michael Dub (auth.), Michael Dub (eds.)
The target of this compilation has been to supply a entire, non-criti cal resource of knowledge touching on organometallic compounds. The scope is proscribed to the compounds containing no less than one carbon-metal bond. The in formation comprises tools of guidance, homes, chemical reactions, and purposes. the 1st variation comprised the literature from 1937 to 1958. the second one variation is totally revised and prolonged via 1964. The literature sooner than 1937 used to be completely lined by way of E. Krause and A. von Grosse in I~ie Chemie der meta11-organischen Verbindungen, " Verlag von Gebrueder Borntraeger, Berlin, 1937. Our paintings comprises 3 volumes. quantity I comprises derivatives of the transition metals of teams III via VIII of the Periodic desk. quantity II includes derivatives of germanium, tin, and lead. quantity III includes derivatives of arsenic, antimony, and bismuth. The compilation is predicated on searches via Chemical Abstracts. The col lection of references for 1964 used to be accomplished ahead of the topic Indexes to Volumes 60 and sixty one of the Abstracts have been to be had; hence a few omissions within the assurance of that yr are attainable. we've tried to make the insurance of the literature whole so that the compilation can have most sensible software to the chemist, chemical engineer, patent legal professional, and editor. within the curiosity of brevity, sure numerical facts are passed over, yet references to the unique literature are given. Yield information are rounded to 2 major figures. at any place attainable, tables were used. The entries within the Bibliography part contain references to Chemical Abstracts.
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Extra info for Compounds of Arsenic, Antimony, and Bismuth: Covering the Literature from 1937 to 1964
By dissolving Re in 30% BaOa, evapg. to dryness, dissolving the residue in coned. HCl and treating the soln. with (Ars) in AcOH; IR spectrum (2042). [Re(O) (Ars)aBrs], yellow microcrystals, prepd. in the same manner as the trichloro complex by using coned. HBr instead of HCl; IR spectrum (2042). [Rh(Ars)a(CO)Cl], yellow prisms, dec. 242-245°, prepd. from [Rh(CO)aC1]a by treating with (Ars) in CaRs (1252, see also 541). [Rh(Ars)a(CO)Cls], yellow crystals, m. ) (1254), dec. 250-255° (1253), prepd.
A curing agent for epoxy resins (1132). A catalyst for the condensation of silanes with unsatd. nitriles (1394). A catalyst for the rxn. of CHa=CHCH2Br with Sn (151'~). In a combination with AlBrs and VBrs catalyzed the polymerization of Ca~ (1608). An antiwear additive for lubricants (1615). A catalyst for the synth. of polyesters (1880). In a combination with TiCls and BusAlaCls catalyzed a stereospecific polymerization of olefins (1473). In a combination with RsAl and Ti trihalides catalyzed the polymerization of olefins (1832).
Soly. data (1052). [Pt(AsEts)2[C(S)(NH2)2]2}I2, the cis and trans isomers were prepd. from the corr. [Pt(AsEt3)212] isomers by dissolving in aq. urea. Soly. data (1052). [Rh(AsEt3)3C13], cis isomer: yellow needles, m. ); trans isomer: red prisms, m. 5°. Both isomers were prepd. from RhC13·3H20 by heating with EtsAs in boiling EtOH. The more sol. trans form was extracted with CsRs from the rxn. mixt. (2167). [Rh(AsEt3)2C1312, orange-brown prisms, m. ); a dinuclear complex with 2 Cl bridges between the Rh atoms, prepd.
Compounds of Arsenic, Antimony, and Bismuth: Covering the Literature from 1937 to 1964 by Michael Dub (auth.), Michael Dub (eds.)